Method of preparing dibenzothiazolyl disulfides

Details Method of preparing dibenzothiazolyl disulfides Method of preparing dibenzothiazolyl disulfides

1977-11-17

1979-03-06

Rizzo, Nicholas S.

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

C07D27778

Patent

active

041430450

ABSTRACT:
Method of preparing dibenzothiazolyl disulfides by oxidizing mercaptobenzothiazole in a substantially neutral saturated aliphatic alcohol solution with a hydroperoxide. The invention has particular utility by providing a relatively pollution-free method of preparing dibenzothiazolyl disulfides.

REFERENCES:
patent: 2024567 (1935-12-01), Clifford
patent: 2593761 (1952-04-01), Johnstone
patent: 3925401 (1975-12-01), Janin
Field et al., JACS, vol. 80, 838, 841(1958).
Osttenberg, Cancer Research 28, 2539-2541(1968).

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