Method of preparing a freeze-dried formulation containing a drug

Drying and gas or vapor contact with solids – Apparatus – With means to treat gas or vapor

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34 15, 34 92, F26B 506

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active

050440918

ABSTRACT:
In a freeze-drying method for producing a dried pharmaceutical compound or preparation, a first liquid is frozen, a second liquid is added to the frozen first liquid and is frozen thereon, and the frozen first and second liquids are freeze-dried together, in which at least one of said first and second liquids contains said pharmaceutical compound of preparation dissolved or suspended therein. The other liquid or liquids may be pure solvent (generally water) or may contain one or more other substances.

REFERENCES:
patent: 4430807 (1984-02-01), Davis et al.
patent: 4433558 (1984-02-01), Cheng et al.
patent: 4470202 (1984-09-01), Buxton et al.
Williams et al., "The Lyophilization of Pharmaceuticals: A Literature Review", J. Parenteral Science and Technology, 38, pp. 48-59 (1976).
Koyama et al., "Effect of Solvent Addition and Thermal Treatment on Freeze Drying of Cefazolin Sodium", J. Parenteral Science and Technology, 42, pp. 47-52 (1988).
Journal of the Research Society of Freezing and Drying, 22, pp. 48-55 (1976).
Farumashi, 5, pp. 99-102, vol. 5, No. 2, Feb. 1969.

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