Method of preparing a cathode by high and low temperature electr

Chemistry: electrical and wave energy – Processes and products

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204 40, 204 43R, 204 43N, 204 43S, 204 43T, 204 43Z, 204 44, 204291, 204293, 204294, C25D 548, C25B 1106, C25B 1108, C25D 356

Patent

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043315178

ABSTRACT:
Disclosed is a method of forming a cathode by electroplating a sacrificial metal and a catalytic metal from an electroplating solution onto an electroconductive substrate. Initial electrodeposition is carried out at a high temperature to preferentially electroplate the catalytic metal, the electroplating solution is then cooled, and thereafter the electrodeposition is carried out at a lower temperature to codeposit sacrificial metal and catalytic metal. Also disclosed is an electrode prepared thereby.

REFERENCES:
patent: 3272728 (1966-09-01), Hahndorf
patent: 4104133 (1978-01-01), Brannan et al.
patent: 4221643 (1980-09-01), Miles et al.
patent: 4250004 (1981-02-01), Miles et al.
Malkin et al., "Reduction of Hydrogen Overpotential in a Chlorine Cell", May, 1979.

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