Chemistry of carbon compounds – Miscellaneous organic carbon compounds – C-metal
Patent
1974-12-18
1976-06-15
Morgenstern, Norman
Chemistry of carbon compounds
Miscellaneous organic carbon compounds
C-metal
260566A, C07C 4500
Patent
active
039637816
ABSTRACT:
A method of preparing 2-hydroxy-3-alkyl-2-cyclopenten-1-one which comprises reacting 2-alkyl-5-carboalkoxycyclopentanone with nitrite in the presence of water and alkali; rendering the reaction system acidic; and either treating the mass for hydrolysis by heating or carrying out oxime exchange reaction in the presence of an aliphatic lower carbonyl compound added as an acceptor to the acidified reaction system.
REFERENCES:
geissman et al., "J. Org. Chem.", vol. 11, pp. 771-772 (1946).
Weygand, "Preparative Org. Chem.," 4th ed., p. 349, (1972).
Kyomori Hiroyuki
Sasaki Kazuhiro
Takahashi Mitsuhiro
Kobayashi Perfumery Co., Ltd.
Morgenstern Norman
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