Method of preparation of 6-aza uracile and its O-disilyl derivat

Details Method of preparation of 6-aza uracile and its O-disilyl derivat Method of preparation of 6-aza uracile and its O-disilyl derivat

1975-10-24

1976-09-28

Ford, John M.

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

C07D25306

Patent

active

039831140

ABSTRACT:
A method of preparation of 6-aza uracile, comprising the steps of:
A. Cyclization of semi-carbazone of glyoxylic acid by heating this latter with an excess of a trialkyl-silylation agent taken as a solvent and isolating the resulting product, namely the O-disilylated derivative of 6-aza uracile (or di-3,5 (trialkylsiloxy)1,2,4 triazine) and
B. subjection of the product resulting from step a) to an acid hydrolysis.

REFERENCES:
patent: 3922273 (1975-11-01), Deutsch

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