Method of performing a chemical reaction

Details Method of performing a chemical reaction Method of performing a chemical reaction

1983-08-05

1984-11-13

Niebling, John F.

Chemistry: electrical and wave energy

Processes and products

204 72, 204 59R, C25B 302

Patent

active

044824386

ABSTRACT:
A streamline flow of aqueous cobalt (II) sulphate solution passes through a platinum tube which, as an anode, electrolyses the solution to cobalt (III). The flow, with a high surface concentration of nascent cobalt (III), falls into a volume of 1-methylnaphthalene in an organic solvent, and is recovered from underneath for recycling to the platinum tube anode.
The cobalt (III) reacts with the 1-methylnaphthalene to form 1-naphthaldehyde. Other oxidations of organic reactants using nascent high-oxidation-state aqueous metal ions are also disclosed.

REFERENCES:
patent: 3953305 (1976-04-01), Connolly
patent: 4329208 (1982-05-01), Vayenas
Clark et al., "Chemistry in Britian" Feb. 1975 (pp. 59-64).

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