Measuring and testing – With fluid pressure – Porosity or permeability
Reexamination Certificate
2006-04-28
2009-08-04
Rogers, David A. (Department: 2856)
Measuring and testing
With fluid pressure
Porosity or permeability
C073S037000, C438S007000, C438S014000, C438S016000
Reexamination Certificate
active
07568379
ABSTRACT:
The method for measuring the porosity of an element is performed by means of a measuring device comprising a measuring chamber in which the element is disposed, a solvent tank associated with an adsorption valve, and a pump associated with a desorption valve. The measuring method comprises measurement of the pressure in the chamber by means of a pressure sensor, and a cycle for measuring the porosity by ellipsometry at different predetermined pressure. During this measuring cycle, a pressure controller controls opening of the adsorption and desorption valves according to the measured pressure. The relative pressure in the chamber is successively regulated at different predetermined values, while maintaining a continuous flow of solvent in the chamber between the tank and the pump.
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Baklanov et al., “Determination of pore size distribution in thin films by ellipsometric porosimetry,”Journal of Vacuum Science and Technology B: Microelectronics Processing and Phenomena, American Vacuum Society, vol. 18, No. 3, May 2000, pp. 1385-1391.
Ferrieu Frédéric
Simon Gurvan
Commissariat a l''Energie Atomique
Oliff & Berridg,e PLC
Rogers David A.
LandOfFree
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