Method of measuring porosity by means of ellipsometry and...

Measuring and testing – With fluid pressure – Porosity or permeability

Reexamination Certificate

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C073S037000, C438S007000, C438S014000, C438S016000

Reexamination Certificate

active

07568379

ABSTRACT:
The method for measuring the porosity of an element is performed by means of a measuring device comprising a measuring chamber in which the element is disposed, a solvent tank associated with an adsorption valve, and a pump associated with a desorption valve. The measuring method comprises measurement of the pressure in the chamber by means of a pressure sensor, and a cycle for measuring the porosity by ellipsometry at different predetermined pressure. During this measuring cycle, a pressure controller controls opening of the adsorption and desorption valves according to the measured pressure. The relative pressure in the chamber is successively regulated at different predetermined values, while maintaining a continuous flow of solvent in the chamber between the tank and the pump.

REFERENCES:
patent: 6319736 (2001-11-01), Baklanov et al.
patent: 6435008 (2002-08-01), Baklanov et al.
patent: 6662631 (2003-12-01), Baklanov et al.
patent: 6831742 (2004-12-01), Sui et al.
patent: 6986280 (2006-01-01), Muckenhirm
patent: 7421885 (2008-09-01), Kitzhoffer et al.
patent: 7458251 (2008-12-01), Baklanov et al.
patent: 2001/0054306 (2001-12-01), Baklanov et al.
patent: 2002/0110921 (2002-08-01), Louwen et al.
patent: WO 03/029789 (2003-04-01), None
Baklanov et al., “Determination of pore size distribution in thin films by ellipsometric porosimetry,”Journal of Vacuum Science and Technology B: Microelectronics Processing and Phenomena, American Vacuum Society, vol. 18, No. 3, May 2000, pp. 1385-1391.

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