Method of measuring hydrogen concentration in member and...

Measuring and testing – Gas analysis – By vibration

Reexamination Certificate

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Reexamination Certificate

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07930925

ABSTRACT:
An art of hydrogen concentration measurement in which the hydrogen concentration of any given location of an object to be measured can be nondestructively obtained is provided.The steps comprises: placing an electromagnetic ultrasonic sensor2in the proximity of, or on, the surface of an object to be measured8, said electromagnetic ultrasonic sensor2generating a magnetic field in which the magnetic flux density changes at high frequency on the wall body of the object to be measured8and receiving a longitudinal ultrasonic wave whose vibration is deflecting in the direction parallel to the thickness direction and a transverse ultrasonic wave whose vibration is deflecting in the direction at an angle of substantially 90° with respect to said longitudinal direction; allowing the electromagnetic ultrasonic sensor2to generate a changing magnetic field so that the longitudinal ultrasonic wave and the transverse ultrasonic wave form a resonant state and receive the longitudinal ultrasonic wave and the transverse ultrasonic wave generated in the object to be measured8; detecting the resonance frequencies of the longitudinal ultrasonic wave and the transverse ultrasonic wave; calculating a predetermined resonance property index using said resonance frequencies of the longitudinal ultrasonic wave and the transverse ultrasonic wave; and calculating the hydrogen concentration of the object to be measured8with reference to a reference material database7which stores the relation between the hydrogen concentration of a member with the same member specifications as those of said object to be measured and the resonance property index.

REFERENCES:
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patent: 2004-101281 (2004-04-01), None
Nakatsuka, M. et al.,“Development of Non-destructive Hydrogen Measurement Method for Fuel Assembly Component Materials”, Atomic Energy Society of Japan, vol. 3, p. 588, 2005.
De. P. K. et al.,“Assessment of Hydrogen Levels in Zircaloy-2 by Non-destructive Testing”, Journal of Nuclear Materials, vol. 252, pp. 43-54, 1998.
Japanese Office Action (with English translation) issued on Feb. 8, 2011, in Japanese Patent Application No. 2005-075702 (5 pages).

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