Method of manufacturing oxide crystal

Superconductor technology: apparatus – material – process – Processes of producing or treating high temperature... – With melting

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505451, 505729, 117 13, 117947, C30B 1502

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active

058519564

ABSTRACT:
A large oxide crystal of high quality is manufactured by increasing the speed of crystal growth without affecting crystal growth. A melt of BaO--CuO as a raw material put in a crucible is heated and melt in the presence of a solid phase precipitate of Y.sub.2 BaCuO.sub.5 and kept at a prescribed temperature. Thereafter, a seed crystal is pulled up while being rotated, with the seed crystal being in contact with the surface of the melt, whereby an oxide crystal having the structure of YBa.sub.2 Cu.sub.3 O.sub.7-x this method, an atmosphere for growing the oxide crystal has an oxygen partial pressure higher than that in an ambient atmosphere.

REFERENCES:
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patent: 5413988 (1995-05-01), Hayashi et al.
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Aoyagi et al., "Effect of oxygen concentration in growth atmosphere on the superconductivity of Bi-Sr-Ca-Cu-O fibers prepared by the micro-czochralski technique", Advanced Superconductivity, Vi, Proc. Int. Symp. Supercond> 6 th (1994) pp. 695-698 abstrac, 1994.

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