Method of manufacturing aromatic urethanes

Organic compounds -- part of the class 532-570 series – Organic compounds – Carboxylic acid esters

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560 25, 560 27, 560 28, 560 30, 560 31, 560 32, C07C26900, C07C27100

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053068424

ABSTRACT:
A method for manufacturing a purified aromatic urethane. Aromatic urethanes are synthesized from a N,N'-disubstituted urea and an organic hydroxyl compound in a reaction medium. The organic hydroxyl compound and the primary aromatic amine side product which are present in the reaction mixture is distilled off and removed from the reaction mixture leaving a distillation bottom. The N,N'-disubstituted urea is separated and removed from the distillation bottom by solvent extraction of the aromatic urethane, and the aromatic urethane in the extract phase obtained in said solvent extraction is separated and purified.

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