Method of manufacturing a silica powder

Chemistry of inorganic compounds – Silicon or compound thereof – Oxygen containing

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423335, 65395, C01B 33157, C01B 3312

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active

060714875

ABSTRACT:
In the method, a suspension of silica particles in water is provided, the suspension is gelled, the resulting gel is dried under microwaves, the dried gel is fractioned into silica granules having a diameter lying in the range 10 .mu.m to 1000 .mu.m, having an apparent density of about 0.5 g/cm.sup.3 to 0.6 g/cm.sup.3, and a porosity of less than 20%, and the granules are screened in the range 100 .mu.m to 500 .mu.m. The suspension in water of silica particles is made by mixing silica soots having a size of less than 0.1 .mu.m and silica grains having a size greater than 1 .mu.m. Its maximum concentration in total weight is greater than that of a suspension of synthetic soots on their own, thereby making it possible to increase the production capacity of the method. Advantageously, the out-of-range granules rejected by the screening are recycled as silica grains for the aqueous suspension, thereby making it possible to increase the accumulated production efficiency of the method.

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Clasen, "Preparation of High-Purity Silica Glass Tubes by Centrifugal Casting of Colloidal Gels", J. of Materials Science Letters 7(1988) pp. 477-478 (No Month).
Clasen, "Preparation and Sintering of High-Density Green Bodies to High Purity Silica Glasses", J. of Non. Crystalline Solids 89(1987) 335-344 (No Month).

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