Method of manufacturing a reference electrode

Chemistry: electrical and wave energy – Apparatus – Electrolytic

Reexamination Certificate

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C427S244000

Reexamination Certificate

active

07744736

ABSTRACT:
A method of manufacturing a reference electrode which has a shaft into which a diaphragm body of a porous ceramic is incorporated is comprised of the following method steps: Impregnating the ceramic with a lyogel precursor prior to incorporating the ceramic body into the shaft, and subsequently transforming the lyogel precursor into a lyogel, from which the solvent is removed through a drying process. A reference electrode has a shaft that is filled with electrolyte, and a diaphragm body formed of a porous ceramic and containing a system of hollow spaces is incorporated into the wall of the shaft. The system of hollow spaces is filled at least partially with a material that is formed of a lyogel by drying and has at least one component that corresponds to the ceramic material.

REFERENCES:
patent: 4170537 (1979-10-01), Simmons
patent: 4711719 (1987-12-01), Leenaars
patent: 0 243 309 (1987-10-01), None
patent: 2 273 672 (1994-06-01), None
patent: 59-107988 (1984-06-01), None
patent: WO 91/12879 (1991-09-01), None
Okubo, et al. “Crack-free porous YSZ membrane via controlled synthesis of zirconia sol” J. Membr Sci 118 (Sep. 18, 1996) 151-157 (EPO Doc XP-002261486).
Anonymous, “Gels”, Internet article (EPO Doc XP-00226187).

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