Method of making titanium disulfide

Details Method of making titanium disulfide Method of making titanium disulfide

1975-12-17

1978-01-17

Cooper, Jack

Chemistry of inorganic compounds

Sulfur or compound thereof

Binary compound

C01G 2300, C01B 1700

Patent

active

040693015

ABSTRACT:
Metallic titanium and a stoichiometric excess of elemental sulfur are reacted at a temperature above about 630.degree. C. but below the critical temperature of elemental sulfur under superatmospheric pressures sufficiently great to insure the presence of molten elemental sulfur to produce titanium disulfide. Upon completion of the reaction, the titanium disulfide is cooled rapidly from at least about 630.degree. C. to minimize formation of titanium trisulfide and titanium disulfide is then separated from the elemental sulfur.

REFERENCES:
patent: 3079229 (1963-02-01), Garrett
patent: 3342552 (1967-09-01), Niermann
Jennin et al., "Compt. Rend" 248, 2875-2877, 1959.
Kenichiro et al., "Chem. Abstracts", vol. 80, 1974, p. 86551s.

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