Method of making polyimide foam structures of controlled density

Adhesive bonding and miscellaneous chemical manufacture – Methods – Surface bonding and/or assembly therefor

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1563073, 1563311, 1563315, 264137, 264321, 521184, 521185, 521189, 521918, B32B 3106

Patent

active

047801670

ABSTRACT:
A method of making structural panels having a controlled density polyimide core, generally with at least one face sheet. An open cell polyimide foam panel is impregnated with a liquid polyimide precursor, compressed to squeeze out all but a desired quantity of the polyimide precursor and dried. One or two face sheets are impregnated with the same liquid polyimide precursor and placed on one or both faces of the foam panel, with pre-drying of the face sheet if desired. This assembly is placed in a mold and subjected to slight compression. The assembly is heated to a moderate temperature for a suitable time to take on the mold configuration. Then the assembly is heated to the curing temperature of the polyimide precursor for a period sufficient to cause curing. The resulting structural panel has a selected density, which determines strength and rigidity, weight and other physical characteristics, controlled by the amount of precursor allowed to remain after the impregnation foam compression step.

REFERENCES:
patent: 4692199 (1987-09-01), Kozlowski et al.
patent: 4715916 (1987-12-01), Shimada

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