Method of making an extremely fine-grained titanium-based carbon

Specialized metallurgical processes – compositions for use therei – Compositions – Consolidated metal powder compositions

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75236, 75239, 75240, 419 10, 419 13, 419 17, 419 18, 419 23, 419 33, C22C 2904

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051375656

ABSTRACT:
According to the present invention there is now provided a method of making a sintered titanium-based carbonitride alloy. According to the method, melt-metallurgical raw materials containing the metallic alloying elements for hard constituent-forming as well as binder phase-forming elements are melted and cast, using no intentional additions of the elements C, N, B and O, to form a pre-alloy which in solidified condition of brittle intermetallic phases with hard constituent-forming and binder phase-forming elements mixed in atomic scale. The pre-alloy is crushed and/or milled to powder with grain size <50 .mu.m. The powder is carbonitrided for simultaneous formation in situ of extremely fine-grained <0.1 .mu.m, hard constituent particles enclosed in their binder phase. The obtained powder is milled together with lubricant and possible additions of powders of metals, carbides and/or nitrides from the groups IV, V or VI in the Periodic Table in order to obtain desired final analysis after which the powder is compacted and sintered.

REFERENCES:
patent: 4783216 (1988-11-01), Kemp et al.
patent: 4894090 (1990-01-01), Ekemar et al.
patent: 4943322 (1990-07-01), Kemp et al.
patent: 5032174 (1991-07-01), Ekemar et al.

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