Method of making .alpha. type silicon nitride powder

Chemistry of inorganic compounds – Silicon or compound thereof – Binary compound

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106 735, C01B 2106

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041170954

ABSTRACT:
.alpha.-Silicon nitride powder which is used as a raw material for the preparation of high strength silicon nitride with additives such as magnesia and yttrium oxide, and other sintered materials suitable for high temperature gas turbine engine components and the like, is prepared by heating a powdered mixture of silica, carbon and metallic silicon in a nitrogen containing atmosphere and then subjecting the material to a heat treatment in an oxidizing atmosphere for decarbonization of said material.

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patent: 3728436 (1973-04-01), Krikorov
patent: 3855395 (1974-12-01), Cutler
patent: 3959446 (1976-05-01), Mazdiyasni et al.
Komeya et al. "J. of Materials Science" 10/1975, pp. 1243-1246.

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