Method of inducing maximum non-linearities into silica for...

Glass manufacturing – Processes of manufacturing fibers – filaments – or preforms – Process of manufacturing optical fibers – waveguides – or...

Reexamination Certificate

Rate now

  [ 0.00 ] – not rated yet Voters 0   Comments 0

Details

C065S111000, C065S425000

Reexamination Certificate

active

06604387

ABSTRACT:

BACKGROUND OF THE INVENTION
This invention relates generally to optical communication, and more particularly the invention relates to a method of treating silica optical fibers and other silica based material using heat and a poling electric field to induce optical non-linearities therein as necessary for optical modulation and switching.
Phase modulators and switches operating in the gigahertz to multigigahertz range are key devices needed for optical communication systems, local area networks, and fiber sensors, in particular in the fiber gyroscope. To date, low voltage phase modulation and switching at reasonably high frequency (>1 MHz) is not available in all-fiber component, of any form. It is typically provided by a LiNbO
3
integrated optic (IO) channel waveguide device, which relies on the electro-optic properties of LiNbO
3
to modulate the phase of the optical signal via an externally applied electric field. These IO devices, however, introduce a relatively high coupling loss, at least 1 dB, when inserted in an optical fiber circuit. The process of physically coupling the IO device to the fiber, called pigtailing, is also costly and difficult. Replacing these IO channel waveguide modulators by an all-fiber modulator would eliminate the high cost and technical difficulties by providing a device which can be directly spliced to the circuit fiber. Splicing would also eliminate altogether mechanical instabilities and undesirable reflection losses which typically occur at a fiber/IO interface.
In the communication area, the loss constraints are even greater. A large portion of the fiber-optical market is projected to be multi-user systems involving hundreds of serial switches, with exceedingly low overall loss, typically under 0.1 dB. Such a stringent requirement again essentially rules out IO components. These considerations practically dictate that these devices must be made in a glass-based fiber. Many other applications will also benefit from the low transmission loss of fiber-based devices in the far IR and UV, and other electro-optic devices, electro-optic fiber modulators and switches can thus be used over a broad range of wavelengths and powers.
SUMMARY OF THE INVENTION
An object of this invention is a new process which will induce a large electro-optic coefficient in glass-based materials, including, but not limited to, standard optical fibers and IO waveguides made in fused silica, and thus make it possible to fabricate low-voltage electro-optic phase and amplitude modulators and switches in a single-mode fiber. Like their IO counterpart, these devices will be driven directly by a low voltage, low current electrical signal.
Briefly, a silica optical fiber or other glass based material is placed in an oven within an enclosure which is preferably a vacuum chamber. Temperature in the oven is ramped from room temperature to a maximum value T
1
, which is on the order of 450° C. or higher. The temperature is ramped at a rate which will not physically damage the glass material. An electric field is applied to the silica material either during the temperature ramping or after the maximum temperature is reached. The field should be as high as possible, on the order of 800 V/&mgr;m or higher, and/or the voltage should be as high as possible (10 kV or higher), without exceeding the dielectric breakdown of the material. The temperature and electric field are maintained for a period of time (poling time) which is in the range of seconds to several tens of minutes. The temperature is then ramped down at a rate slow enough to allow the material to be in constant poling equilibrium. The voltage is switched off when the temperature of the sample has dropped to a low enough value, ideally room temperature (typically 20° C.) although higher temperatures (such as 50° C.) may be also suitable.
The invention including processing alternatives will be more readily apparent from the following description and appended claims when taken with the drawings.


REFERENCES:
patent: 2897126 (1959-07-01), George
patent: 3681041 (1972-08-01), D'Huart
patent: 3850603 (1974-11-01), Drake
patent: 3880630 (1975-04-01), Izawa
patent: 4557742 (1985-12-01), Thigpen
patent: 5127928 (1992-07-01), Farries et al.
patent: 5237576 (1993-08-01), DiGiovanni
patent: 5401003 (1995-03-01), Aizatulov
patent: 5436758 (1995-07-01), Agostinelli et al.
patent: 5617499 (1997-04-01), Brueck et al.
patent: 5676587 (1997-10-01), Landers
patent: 5777432 (1998-07-01), Xie
patent: 5907652 (1999-05-01), DiGiovanni
patent: 6001470 (1999-12-01), Niwa
patent: WO 90/08970 (1990-01-01), None
patent: WO 95/29425 (1995-04-01), None
M.C. Farries and A.J. Rogers, Temperature Dependence of the Kerr Effect in Silica Optical Fibre,Electronics Letters, vol. 19, No. 21, 13thOct. 1983, pp. 890-891.
U. Österburg and W. Margulis, Dye laser pumpled by Nd: YAG laser pulses frequencey doubled in a glass optical fiber,Optics Letters, vol. 11, No. 8, Aug. 1986, pp. 516-518.
D.M. Krol and J.R. Simpson,Photoinduced second-harmonic generation in rare-earth-doped aluminosilicate optical fibers, Optics Letters, vol. 16, No. 21, Nov. 1, 1991, pp. 1650-1652.
R.A. Myers, N. Mukherjee, and S.R.J. Brueck, Large second-order nonlinearity in poled fused silica,Optics Letters, vol. 16, No. 22, Nov. 15, 1991, pp. 1732-1734.
J.F. Valley, J.W. Wu, S. Ermer, M.Stiller, E.S. Binkley, J.T. Kenney, G.F. Lipscomb, and R. Lytel,Thermoplasticity and parallel-plate poling of electro-optic polyimide host thin films, Applied Physics Letters, vol. 60, No. 2, Jan. 13, 1992, pp, 160-162.
T. Fujiwara, D. Wong, Y. Zhao, S. Fleming, S. Poole, and M. Sceats, Electro-OpticEffect Induced by UV-Excited Poling in a Silica Fibre,19thAustralian Conference on Optical Fiber Technology, Postdeadline Paper PDP-3 (1994).
U. Österburg and W. Margulis, Dye laser pumped by Nd: YAG laser pulses frequency doubled in a glass optical fiber,Optics Letters, vol. 11, No. 8, Aug. 1986, pp. 516-518.
Richard A. Myers and S.R.J. Brueck,Stable Second-Order Nonlinearity in SiO2-Based Waveguides on Si Using Temperature/Electric Field Poling, Doped fiber devices and systems, SPIE 2289, San Diego, Jul. 1994, pp. 1-3.
P.G. Kazansky and P. St.J. Russell,Thermally poled glass: frozen-in electric field or oriented dipoles?, Optical Communication, vol. 110, Sep. 1, 1994, pp. 611-614.
X.-C. Long, R.A. Myers, and S.R.J. Brueck,Measurement of linear electro-optic effect in temperature/electric-electric field poled optical fibres, Electronics Letters, vol. 30, No. 25, 8thDec. 1994, pp. 2162-2163.
L.E. Myers, R.C. Eckardt, M.M. Fejer, R.L. Beyer, W.R. Bosenbert, and J.W. Pierce,Quasi-phase-matched optical parametric oscillators in bulk periodically poled LiNbO3,Journal of the Optical Society of America B.(Optical Physics), vol. 12, No. 11, Nov. 1995, pp. 2102-2116.
P.G. Kazansky, A.R. Smith, L. Dong, P. St.J. Russell,Second harmonic generation in silica fibers poled via internal electrodes, Conference on Lasers and Electro-Optics 1996(CLEO'96), Paper CWK2 (Jun. 1996).

LandOfFree

Say what you really think

Search LandOfFree.com for the USA inventors and patents. Rate them and share your experience with other people.

Rating

Method of inducing maximum non-linearities into silica for... does not yet have a rating. At this time, there are no reviews or comments for this patent.

If you have personal experience with Method of inducing maximum non-linearities into silica for..., we encourage you to share that experience with our LandOfFree.com community. Your opinion is very important and Method of inducing maximum non-linearities into silica for... will most certainly appreciate the feedback.

Rate now

     

Profile ID: LFUS-PAI-O-3086431

  Search
All data on this website is collected from public sources. Our data reflects the most accurate information available at the time of publication.