Method of forming polymer particles

Plastic and nonmetallic article shaping or treating: processes – Formation of solid particulate material directly from molten... – Utilizing centrifugal force or rotating forming zone

Reexamination Certificate

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Reexamination Certificate

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11178091

ABSTRACT:
The present invention is a method of manufacturing polymer particles. The method includes providing an oil in water emulsion, wherein the oil phase comprises a volatile solvent and at least one water insoluble polymer. The volatile solvent has a solubility of not more than 10% in water and the water insoluble polymer has a weight average molecular weight of at least 2000. The water insoluble polymer is soluble in the volatile solvent. The emulsion is supplied to a rotating surface of a rotating surface reactor. The temperature of the rotating surface is maintained at the boiling point of said solvent or greater. The rotating surface of the reactor spins at a speed sufficient to cause the emulsion to spread over the rotating surface as a continuously flowing thin film wherein a vapor phase containing the volatile solvent is removed. The water insoluble polymer particles are then collected as a slurry of polymer particles and water.

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R.J.J. Jachuck et al., “Process Intensification: Removal of an Organic Component From an Aqueous Emulsion Using Spinning Dis Reactor Technology”, Heat Recovery Systems and CHP, 1994, vol. 14, No. 5, pp. 475-491.

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