Method of forming nanostructures on ceramics

Plastic and nonmetallic article shaping or treating: processes – Outside of mold sintering or vitrifying of shaped inorganic... – Controlling or directing flow of heated gas or exhaust...

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C977S763000

Reexamination Certificate

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10678772

ABSTRACT:
A method for manufacturing oriented arrays of ceramic or metal oxide nanostructures, such as titania (TiO2) nanofibers. The nanofibers are formed on the surface of a body that is first sintered at a temperature in the range of about 1,100 to about 1,400 degrees Celsius. Subsequently, the surface is exposed to an H2-bearing gas, such as H2and N2in a ratio of about 5:95 at about 700 degrees Celsius for about 8 hours. During heat treatment in the gas phase reaction, sintered titania grains transform into arrays of nanofibers oriented in the same crystallographic direction.

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