Method of forming improved tungsten ingots

Powder metallurgy processes – Powder metallurgy processes with heating or sintering – Consolidation of powder prior to sintering

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419 23, 419 42, 419 58, 75248, B22F 100

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050193309

ABSTRACT:
A method of forming tungsten ingots having improved uniformity of density and improved uniformity in distribution of dopant within the ingot is disclosed. Doped tungsten powder is disposed in a cylindrical mold having sealing means at both ends. The powder completely fills a void space within the mold between the sealing means so that there is substantially no settling of the powder. A pressure of about 560 kg/cm.sup.2 is applied uniformly to the outer surface of the mold to form a cylindrical compact. The compact is removed from the mold and resistance sintered to a density of at least about 85 percent of theoretical density to form the ingot.

REFERENCES:
patent: 3443143 (1969-05-01), Koo
patent: 3661536 (1972-05-01), Shimizu et al.
patent: 3838486 (1974-10-01), Millner et al.
patent: 3853492 (1974-12-01), Millner et al.
patent: 3927989 (1975-12-01), Koo
patent: 4931252 (1990-06-01), Brunisholz
"The Application of Tungsten Wire as the Light Source in Incandescent Electric lamps", D. J. Jones, Metallurgy and Material Technology, vol. 5, No. 10, pp. 503-512, 1973.
"Tooling for Cold Isostatic Pressing", Isostatic Pressing Technology, Applied Science Publishers, New York, edited by P. J. James, 1983, Chapter 4, pp. 90-123 & 160-161.

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