Method of forming fine dispersion of ceria in tungsten

Powder metallurgy processes – Powder metallurgy processes with heating or sintering – Metal and nonmetal in final product

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419 19, 419 38, 419 45, 75359, 75361, 75365, B22F 924

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active

052846148

ABSTRACT:
Doped tungsten powder, or sintered tungsten bodies formed therefrom, having a fine dispersion of oxide particles of at least one metal from the group zirconium, hafnium, lanthanum, yttrium, and rare earth's are formed by the method of this invention. A mixture of a salt solution comprised of a soluble salt of the metal, and a tungsten blue oxide powder is formed. A hydroxide precipitating solution is admixed with the mixture to form a hydroxide precipitate of the metal on the tungsten blue oxide powder. The tungsten blue oxide powder and hydroxide precipitate are heated in a reducing atmosphere to form the tungsten powder having the dispersion of oxide particles. The doped tungsten powder can be consolidated and sintered to form tungsten bodies having a fine dispersion of the metal oxide.

REFERENCES:
patent: 3475159 (1969-10-01), hansen
patent: 4156053 (1979-05-01), Baranow
patent: 4678718 (1987-07-01), Wang
patent: 4787561 (1988-11-01), Kemp et al.
patent: 4923673 (1990-05-01), Litty

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