Method of fabricating silica-titania nanoporous composite...

Compositions – Compositions containing a single chemical reactant or plural... – Inorganic reactant other than sulfur containing

Reexamination Certificate

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C252S520200, C252S521300, C524S001000, C524S080000, C524S081000, C523S527000

Reexamination Certificate

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08070981

ABSTRACT:
Provided is a method of fabricating silica-titania nanoporous composite powder by controlling a pore size. In more particular, a method of fabricating silica-titania nanoporous composite powder, using a spraying and heating reactor including an ultrasonic droplet generator and a cylindrical electric furnace, comprises the steps of: generating droplets of a mixture suspension from a colloidal suspension prepared by mixing silica (SiO2) and titania (TiO2) nanopowders and organic template (PSL: polystyrene latex) powder, by the ultrasonic droplet generator of the spray-heating reactor; generating a silica-titania-organic template nanoporous composite powder having pores within the range of 20˜100 nm in size through preparing silica-titania-organic template (SiO2—TiO2-PLS) composite particles and removing the organic template while passing the mixture suspension in the cylindrical electric furnace by a carrier gas; and collecting the generated nanoporous material by a particle collector.

REFERENCES:
patent: 2009/0000651 (2009-01-01), Qiao
patent: WO 2009/016143 (2009-02-01), None
patent: WO 2009/032988 (2009-03-01), None
Gi-Ra Ti, Ordered Macroporous Particles by Colloidal Templating May 24, 2004, Chem. Mater. 2001, 13, 2613-2618.

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