Glass manufacturing – Processes of manufacturing fibers – filaments – or preforms – With measuring – controlling – sensing – programming – timing,...
Reexamination Certificate
2000-03-06
2004-04-06
Hoffmann, John (Department: 1731)
Glass manufacturing
Processes of manufacturing fibers, filaments, or preforms
With measuring, controlling, sensing, programming, timing,...
C065S421000, C065S391000, C065S404000, C065S484000
Reexamination Certificate
active
06715321
ABSTRACT:
BACKGROUND OF THE INVENTION
1. Field of the Invention
The present invention relates to a method of fabricating an optical fiber preform including a step of outside deposition of silica possibly doped with at least one dopant by injecting at least one substance in the form of silica or a precursor of silica in the vicinity of a heating area created by heating means during at least one pass of injector means and the heating means along a longitudinal axis of the preform. It also relates to a preform obtained by the above method and an optical fiber fabricated by drawing the above preform.
2. Description of the Prior Art
Using an outside lateral deposition technique such as the plasma surfacing technique to fabricate a preform, which is subsequently drawn to fabricate an optical fiber, from another preform referred to as the primary preform, which includes the optical guide part of the optical fiber obtained from the preform, is known in the art and described in patent application EP 0 450 465 A1, for example.
The optogeometrical characteristics of an optical fiber determine transmission characteristics. They include the geometry of the fiber, in particular the surfaces of the various concentric parts of the fiber when seen in cross section, and the optical characteristics of these various parts. These optogeometrical characteristics are derived from those of the preform from which the optical fiber is fabricated.
Patent application EP 0 719 738 A1 describes a method of obtaining optical fiber preforms using a plasma surfacing process, i.e. an outside deposition process using a plasma torch as the heating means, in which method silica, possibly doped silica, and generally in the form of grains of silica, is injected into the torch and at least one plasma surfacing pass is modulated to improve the optogeometrical properties of the preform. The surfacing pass which is modulated is one of the final surfacing passes; during unmodulated passes the thickness of the surfacing layer deposited is substantially constant along the usable port of the preform. The surfacing process is modulated principally by controlled axial modification of at least one plasma surfacing parameter, preferably the flowrate of the surfacing grains. The axial modification process includes evaluating axial diameter errors of the preform and axially modifying the parameter in a direction such that the modulated surfacing pass reduces the axial diameter errors. In other words, the surfacing pass is modulated according to axial diameter errors previously determined and adds to—or subtracts from—the diameter of the preform so that the errors are reduced—or even eliminated—after the surfacing pass.
However, in patent application EP 0 719 738 A1 the outside deposition yield is not optimized: the injector means, in this instance for injecting grains, are permanently positioned relative to the plasma torch throughout the duration of outside deposition. The heating means (the plasma torch). do not operate symmetrically about their axis on the reactive gases or particles leaving the injector means, principally because of the vortex flow of the plasma gases in the torch and at the outlet from the torch. Consequently, in an outside deposition process alternating deposition passes in opposite directions, the position of the injector means in the prior art typically represents a compromise. Its position is between an optimum position in one direction of translatory movement of the preform and an optimum position in the other direction of translatory movement of the preform. Consequently, the outside deposit is not optimized, in particular in terms of the yield; the reactive gases or grains leaving the injector means and which have not reacted in the heating area of the heating means are purely and simply eliminated without having been able to react.
With a process of the above kind it is also difficult to deposit doponts such as fluorine with some rates of incorporation into the preform. The position of the injector means can make it impossible to obtain correct doped reactant deposition reaction kinetics, principally in terms of temperature and the distance to be traveled by the reactants leaving the injector means if the reactants are gases. Fluorine, for example, is too reactive and, instead of silica and fluorinated substance being deposited on the preform, an unwanted compound SiF
4
is formed which is not incorporated into the preform. In the worst case scenario not only is the fluorine dopant not incorporated into the preform but it also impedes or even prevents the deposition of silica on the preform.
In the context of the outside vapor deposit (OVD) technology, in which an outside deposit of possibly doped silica is produced by a succession of outside deposit passes of soot in the presence of the heating means, which are generally in the form of an oxyhydride torch, vitrification occurring after such deposition, generally in an oven, the problem also arises of optimizing the outside deposit, in, addition to the problem of depositing some doponts under some conditions. It is also feasible to form an OVD deposit by using a plasma torch as the heating means instead of an oxyhydride torch.
The method of the invention aims principally to increase the deposition yield of the outside deposit process by optimizing the position of the injector means relative to the heating means. It also aims to enable simultaneous deposition of doponts and silica under good conditions.
SUMMARY OF THE INVENTION
The invention provides a method of fabricating an optical fiber preform including a step of outside deposition of silica possibly doped with at least one dopant by injecting at least one substance in the form of silica or a precursor of silica in the vicinity of a heating area created by heating means during at least one pass of injector means and the heating means along a longitudinal axis of the preform during which the relative positions of the injector means and the heating means are adjusted so that the silica is deposited in the heated area regardless of the position of the heating means.
In the case of direct vitrification, where possibly doped silica soot is deposited and the soot is simultaneously vitrified, it is very important to obtain a good quality preform, and in particular for no bubbles to be incorporated in the preform. While significantly improving the silica deposition yield, generally by 20% to 30% compared to a compromise position of the injector means, the method of the invention has the advantage of producing a high-quality deposit essentially free of bubbles.
The method according to the invention also has the advantage, principally in the case of injecting gaseous reactants, of obtaining some levels of dopants in the silica deposited by the surfacing process which a standard position of the injector means cannot achieve well, if at all.
The adjustment is advantageously carried out at each change of pass.
The method of the invention therefore has the advantage, principally in the case of depositing grains in both surfacing pass directions, at constant deposit quality, of increasing the rate of deposition of the particles deposited on the preform in a lateral surfacing layer, compared to the process in which the injector means are fixed at a particular position throughout the surfacing process.
In one embodiment of the invention the heating means have a main axis in a plane substantially perpendicular to the longitudinal axis of the preform, the injector means have a main axis at a fixed angle to the main axis of the heating means in a plane substantially perpendicular to the longitudinal axis of the preform and the injector means and the heating means move relative to each other in a direction parallel to the longitudinal axis of the preform.
In this configuration the orientations of the principal axes of the injector means and the heating means are conventional for the process of outside deposition of possibly doped silica, principally in the case of plasma surfacing, and the method of the invention can easily
Drouart Alain
Gouez Benoît
Ripoche Pierre
Alcatel
Hoffmann John
Sughrue & Mion, PLLC
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