Method of estimating preferred orientation of...

X-ray or gamma ray systems or devices – Specific application – Diffraction – reflection – or scattering analysis

Reexamination Certificate

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Reexamination Certificate

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06873681

ABSTRACT:
The preferred orientation of a polycrystalline material is estimated using one diffraction peak. An orientation density distribution function ρ is assumed to be axisymmetric around a normal direction of the surface of a sample made of a polycrystalline material. The function ρ may be a Gaussian function or a March-Dollase function. An X-ray is incident upon the surface of the sample at an incident angle α and the intensity of a diffraction X-ray is measured. The change of intensity of the diffraction X-ray is measured with the incident angle α being changed to attain a measurement rocking curve. A theoretical diffraction X-ray intensity is calculated based on the orientation density distribution function ρ. The characteristic parameter of the function ρ is determined so that the theoretical rocking curve approaches the measurement rocking curve as closely as possible, whereby the orientation density distribution function ρ can be determined.

REFERENCES:
patent: 05-001999 (1993-01-01), None
James, R. W., “The Optical Principles of the Diffraction of X-Rays.” G. Bell and Sons LTD., London, (1967), pp. 34-52.
Dollase, W.A., “Correction of Intensities for Preferred Orientation in Powder Diffactometry: Application of the March Model.” J. Appl. Cryst. (1986), vol. 19, pp. 267-272.
Seabaugh M, M., et al., “Comparison of texture analysis techniques for highly oriented alpha-A1203” Journal of the American Ceramic Society, vol. 83, No. 8, Aug. 2000, pp. 2049-2054, XP002299301 USA.
Vaudin M. D., et al., “A method for crystallographic texture investigation using standard s-ray equipment” Journal of Materials Research, vol., 13, No. 10, Oct. 1998, pp. 2910-2919, XP002299493 USA.
Neerinck, D. G., et al. “Depth Profiling of thin Ito films by grazing incidence x-ray diffraction” Thin Solid Films, Elselvier-Sequoia S.A. Lausanne, CH, vol. 278, No. ½, May 15, 1996, pp. 12-17, XP000637212, ISSN: 0040-6090.

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