Method of determining elements in metals by means of optical emi

Optics: measuring and testing – By dispersed light spectroscopy – With sample excitation

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G01N 2167

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045926557

ABSTRACT:
Contents of elements in metals, e.g. aluminum in steel, which are present as a total quantity in an elemental/dissolved form and in a non-elemental or separated form, are determined by sparking the surface of the metal under an inert atmosphere. The spectral signal is simultaneously measured as a function of time, and a signal is obtained which initially exhibits an intensity peak, from which the non-elemental or separated element content can be concluded, and the signal then stabilizes at a stationary value from which the total content (C.sub.t) of element can be concluded. The elemental/dissolved proportion (C.sub.s) can be concluded from the total area (P.sub.1) below the peak, from the area (P.sub.2) under the stationary intensity measured over a time (t.sub.2 -t.sub.1) and from the total content (C.sub.t).

REFERENCES:
patent: 3248602 (1966-04-01), Irish et al.
patent: 3729259 (1973-04-01), Cooper et al.
patent: 3876306 (1975-04-01), Onodera et al.
patent: 3957373 (1976-05-01), Clarke
patent: 4326801 (1982-04-01), Ono et al.

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