Distillation: apparatus – Apparatus – Elements
Reexamination Certificate
2010-08-03
2011-11-15
Monaharan, Virginia (Department: 1771)
Distillation: apparatus
Apparatus
Elements
C106S014120, C106S014210, C159SDIG015, C159SDIG020, C159SDIG021, C203S007000, C203S051000, C203S086000, C252S389200, C568S913000, C034S427000
Reexamination Certificate
active
08057642
ABSTRACT:
This invention relates to a process for reducing the corrosion rate of iron-containing vessels within an ethylene glycol distillation system. The inventive process includes the addition of an additive component of sodium nitrite and sodium hypophosphite into such iron-containing vessels, to thereby react with iron of the inside walls and form a protective coating thereon. This process reduces the corrosion rate in iron-containing vessels of the apparatus, and reduces the catalytic effects of iron corrosion products within the system. Thus, not only is the on-stream time of the vessels extended, but also product quality is improved by reducing the aldehyde content of the final ethylene glycol product.
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Billig Barry
Mann James
Monaharan Virginia
Scully , Scott, Murphy & Presser, P.C.
SD Lizenzverwertungsgesellschaft mbH & Co. KG
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