Method of conducting reactions in a trickle-type reactor

Organic compounds -- part of the class 532-570 series – Organic compounds – Oxygen containing

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C07C 2917

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active

042373255

ABSTRACT:
Trickle-type fixed-bed catalytic reactions are improved, prior to starting or resuming an on-stream period, by purging air from the catalyst bed and reaction zone by downward flow of an inert gas therethrough, flooding the purged reaction zone by flowing a liquid upwardly through the catalyst bed to cover same, then removing the liquid and instituting the on-stream period by introducing gaseous and liquid reactants at the upper end of the catalyst bed to flow downwardly therethrough.

REFERENCES:
patent: 4003952 (1977-01-01), Foster et al.
Hanika et al., Coll. Cyech Comm., vol. 39, pp. 210-215 (1974).
Satterfield A.I.Ch.E. J., vol 21(2), pp. 209-228 (1975).

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