Method of conducting reactions in a trickel-type reactor

Organic compounds -- part of the class 532-570 series – Organic compounds – Oxygen containing

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C07C 4545

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active

042319668

ABSTRACT:
Trickle-type fixed-bed catalytic reactions are improved, prior to starting or resuming an on-stream period, by purging air from the catalyst bed and reaction zone by downward flow of an inert gas therethrough, flooding the purged reaction zone by flowing a liquid upwardly through the catalyst bed to cover same, then removing the liquid and instituting the on-stream period by introducing gaseous and liquid reactants at the upper end of the catalyst bed to flow downwardly therethrough.

REFERENCES:
patent: 3574763 (1971-04-01), Wollner et al.
Satterfield, A I Chem. E. J., vol. 21 (2), pp. 209-228, (1975).

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