Method of annealing/magnetic annealing of amorphous metal in a f

Metal treatment – Process of modifying or maintaining internal physical... – Magnetic materials

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148304, 252 6255, C21D 104, C21D 153

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052250059

ABSTRACT:
A method of heat treating an amorphous metal alloy by immersing the alloy in a fluidized bed to heat the alloy to a temperature below its recrystallization temperature. The alloy is maintained in the fluidized bed for a time sufficient to reduce internal stresses while minimizing crystal growth and nucleation of crystallites in the alloy. Then, the alloy is removed from the fluidized bed and cooled. A magnetic field can be applied to the alloy before, during or after heating the alloy in the fluidized bed. The magnetic field is applied for a time sufficient to achieve substantial magnetic domain alignment while minimizing crystal growth and nucleation of crystallites in the alloy. The cooling step is effective to maintain the magnetic domain alignment in the alloy. The cooling step can be performed with a chill bath or a fluidized bed which is cooled by a circulating gas such as nitrogen or air. The alloy can be slowly cooled by convection and radiation after it is removed from the first fluidized bed.

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