Method of adjusting a fused salt electrolytic bath

Details Method of adjusting a fused salt electrolytic bath Method of adjusting a fused salt electrolytic bath

1977-06-01

1978-09-12

Mack, John H.

Chemistry: electrical and wave energy

Processes and products

C25D 366

Patent

active

041135822

ABSTRACT:
A high valency salt, such as TiCl.sub.4 is reduced to a lower valency salt, such as TiCl.sub.2 and/or TiCl.sub.3 within a fused salt electrolytic bath via electrolysis so that an improved electrodeposition of a desired metal or alloy, such as Ti, occurs, from such adjusted bath. The process generally comprises adding a higher valency salt of a desired metal or alloy to a fused salt electrolytic bath, reducing the higher valency salt on a cathode electrode to a lower valency salt, removing the so-produced lower valency salt from the electrode surface and maintaining a predetermined amount of the lower valency salt within the electrolytic bath. Electrodeposition of a desired metal or alloy may then take place from such electrolytic bath containing a so-adjusted amount of the lower valency salt.

REFERENCES:
patent: 3024174 (1962-03-01), Stetson
patent: 4016052 (1977-04-01), Tokumoto et al.

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