Method for waste recovery from a process of the production of di

Details Method for waste recovery from a process of the production of di Method for waste recovery from a process of the production of di

1977-08-25

1978-12-26

Mars, Howard T.

Organic compounds -- part of the class 532-570 series

Organic compounds

Oxygen containing

568806, C07C 3906

Patent

active

041317491

ABSTRACT:
The essence of the invention consists in heating the dian waste in the presence of sodium hypophosphite as a catalyst in amount of 0.01 - 0.5% by weight at a temperature of 150 to 250.degree. C and under reduced pressure in the range of 5 to 50 mm Hg. As a result a destillate is obtained containing as main components phenol, o- and p-isopropenyl-phenol and their dimers at yield of about 40-74% by weight calculated in relation to the initial amount of dian waste. The distillate obtained was made up with fresh phenol or with phenol and acetone and brought into contact with strongly acid cation exchanger, such as Wofatit KPS, Zerolit 225, Wofatit OK-80, in consequence the o- and p-isopropenylphenol and their dimers reacted with phenol to obtain the dian, the latter being then separated by known methods.

REFERENCES:
patent: 2497503 (1950-02-01), Jones
patent: 3466337 (1969-09-01), Smith et al.

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