Method for the synthesis of borazine

Details Method for the synthesis of borazine Method for the synthesis of borazine

1978-03-30

1979-04-17

Peters, G. O.

Chemistry of inorganic compounds

Boron or compound thereof

Nitrogen and hydrogen containing

C01B 3514

Patent

active

041500970

ABSTRACT:
A method for synthesizing borazine by preparing a liquid mixture of ammonia borane and a high boiling point solvent which is inert to ammonia borane, and heating said mixture to obtain borazine and hydrogen. Volatized borazine is stripped from the hydrogen during synthesis and any borazine entrained in the solvent is removed by distillation.

REFERENCES:
stock, A.; Hydrides of Boron and Silicon; Cornell Univ. Press; Ithaca, N.Y.; 1957; pp. 92-93.
Niedenzu, K. et al., Boron-Nitrogen Compounds; Academic Press, N.Y.; 1965; pp. 86-88.

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