Method for the reduction of allyl alcohols

Details Method for the reduction of allyl alcohols Method for the reduction of allyl alcohols

1995-05-30

1996-12-17

Trinh, Ba K.

Organic compounds -- part of the class 532-570 series

Organic compounds

Heterocyclic carbon compounds containing a hetero ring...

549312, C07D30783

Patent

active

055855016

ABSTRACT:
A method for reduction of an allyl alcohol-type compound, specific to its allylic hydroxyl group, being carried out without any side reactions such as reduction of other portions of the compound or allylic rearrangement, which comprises treating the compound with trialkylsilane in the presence of AlX.sub.3, wherein X refers to a halogen atom.

REFERENCES:
Doyle et al., J. Org. Chem. vol. 41, No. 8, pp. 1393-1396 (1976).
Adlington et al., Tetrahedron Letters, No. 34, pp. 2955-2958 (1976).
Brewster et al., J. Org. Chem. vol. 29, pp. 116-121 (Jan. 1964).
Corey et al., J. Amer. Chem. Soc., vol. 93, No. 6, pp. 1491-1493 (1971).

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