Method for the recovery of furfural, acetic acid and formic acid

Distillation: processes – separatory – Distilling to separate or remove only water – From organic compound

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203 16, 203 17, 203 63, 203 77, 203 91, 203DIG6, 159 473, 162 16, 422197, 422198, 422202, 422206, 549489, 549490, 562513, 562608, 562609, C07C 5144, C07C 5148, C07D30750

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active

044015143

ABSTRACT:
A method of recovering or extracting chemicals, such as furfural, formic acid, acetic acid and other organic compounds from acidic hydrolysates of plants or vegetable matter, especially spent sulfite liquors after conversion of the pentosans into pentoses and then into furfural by heating the hydrolysate in an acidic environment. The conversion of the pentosans pentoses into furfural, preferably with acidulation, is accomplished in a counterflow or countercurrent flow heat exchanger and a reactor, preferably a tubular reactor. The hydrolysate which has additionally been heated and converted in the reactor is used as a heating medium or heat carrier for heating up the hydrolysate which is converted in the counterflow heat exchanger, whereupon there is recovered as the distillate furfural in conjunction with the formic acid, acetic acid and the like.

REFERENCES:
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patent: 4143066 (1979-03-01), Kalcevic
patent: 4143702 (1979-03-01), Barr

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