Method for the production of high-purity triaminotrinitrobenzene

Details Method for the production of high-purity triaminotrinitrobenzene Method for the production of high-purity triaminotrinitrobenzene

1976-07-19

1977-06-28

Engle, Samuel W.

Explosive and thermic compositions or charges

Containing nitrated organic compound

Nitrated aromatic compound

260645, C06B 2504, C07C 7910

Patent

active

040323773

ABSTRACT:
Triaminotrinitrobenzene is readily formed by the nitration of 1,3,5-trichlorobenzene to 1,3,5-trichloro-2,4,6-trinitrobenzene followed by amination to triaminotrinitrobenzene. The purity of the triaminotrinitrobenzene is significantly improved if, during the amination step, sufficient water is present that the byproduct ammonium chloride formed during the amination is rendered at least semideliquescent.

REFERENCES:
patent: 3185738 (1965-05-01), Cossaboon
patent: 3816551 (1974-06-01), Lee
patent: 3985595 (1976-10-01), Benziger
Benziger et al., "Pilot Plant Production of Triaminotrinitrobenezene (TATB)", LA-3632 (LASL).

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