Method for the preparation of sinterable nitrides

Chemistry of inorganic compounds – Nitrogen or compound thereof – Binary compound

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423409, 423410, 423412, 501 96, C01B 21072, C01B 21076, C04B 3558

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049294334

ABSTRACT:
Nitride powders of high surface area, uniform small particle size and high purity are prepared by forming in an aqueous medium a homogeneous combination of a soluble or colloidally dispersible compound of a multivalent metal with a water soluble oxygen oxygenated carbonaceous polymer, e.g., by mixing an aluminum or other metal salt with polyacrylic acid or mixing colloidal hydrated alumina, or other such metal oxide, with a water soluble oxygenated carbonaceous polymer such as sucrose or methyl cellulose. The resulting precipitate or gel is dried and calcined in a nitriding atmosphere, forming a nitride powder which is highly suitable for fabrication of ceramic bodies by sintering at lower than conventional temperatures.

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