Method for the preparation of rhamnose monohydrate from rhamnoli

Organic compounds -- part of the class 532-570 series – Organic compounds – Carbohydrates or derivatives

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536 111, 536128, 127 34, 127 36, C07H 100, C07H 106, C07H 108, C13K 1300

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055502270

ABSTRACT:
The invention relates to a method for the preparation of rhamnose from rhamnolipids, for which an acidic emulsion of the rhamnolipid is hydrolyzed at 100.degree. to 200.degree. and subsequently cooled, the aqueous phase of the resulting hydrolysate is separated from the lipid phase, its pH is raised by the addition of a basic compound, any precipitate formed is removed, the remaining solution is concentrated and either processed further directly or chromatographed on ion exchange resin, rhamnose-containing fractions being obtained as eluate, which are processed further as such or worked up into crystalline rhamnose monohydrate.

REFERENCES:
patent: 4758283 (1988-07-01), Takemura et al.
patent: 4772334 (1988-09-01), Hatanaka et al.
patent: 4814272 (1989-03-01), Wagner et al.
patent: 4933281 (1990-06-01), Daniels et al.
patent: 5077206 (1991-12-01), Cheetham et al.

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