Method for the preparation of N-methyl and -N-ethyl-1-pyrrolidon

Organic compounds -- part of the class 532-570 series – Organic compounds – Heterocyclic carbon compounds containing a hetero ring...

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C07D207267, C07D20727

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044043910

ABSTRACT:
The invention relates to a process for the preparation of a N-alkyl-2-pyrrolidone by reducing the corresponding N-(.alpha.-hydroxyalkyl)-2-pyrrolidone in the liquid phase under an atmosphere of hydrogen gas and in the presence of a noble metal hydrogenation catalyst while in the absence of trifluoroacetic acid.

REFERENCES:
patent: 3073843 (1963-11-01), Buc
patent: 3274211 (1966-09-01), Schmerling
patent: 3821245 (1974-06-01), Kanetaka et al.
Auerbach et al., J. Org. Chem., vol. 41, No. 4, 1976, pp. 725 & 726.
Brennstoff-Chemie, Nr. 5 Bd. 48, pp. 135-139.
Merck Chemical Index, p. 897, (8th Ed. 1968).
Harrison & Harrison, vol. 1, Comp. of Synthetic Methods, pp. 211-212, (1971).
Bernardi et al., J. Chem. Soc. Chem. Comm. 320, (1975).
Johnson and Crosby, J. Org. Chem. 27, 2205, (1962).
Basha et al., Synthetic Communications 7(8), pp. 549-552, (1977).
J. March, Advanced Organic Chemistry, pp. 388-389, (1977).
Kirk-Othmer, Encyclopedia of Chem. Tech., vol. 19, pp. 514, 517-520, (3rd Ed., 1982).

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