Method for the preparation of alcohol-free alkali and alkaline e

Details Method for the preparation of alcohol-free alkali and alkaline e Method for the preparation of alcohol-free alkali and alkaline e

1974-06-25

1976-07-27

Thomas, Jr., James O.

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

260643A, C07C 3130

Patent

active

039718336

ABSTRACT:
A process for the preparation of an alcohol-free alkali or alkaline earth metal alcoholates dissolved in inert solvent which comprises contacting at least an equimolar amount of an alkali or alkaline earth metal dissolved in an inert solvent with an alcohol at an elevated pressure and at a temperature of at least that at which crystal alcohol splits off from the corresponding alkali or alkaline earth metal alcoholate and below the temperature at which said alcoholate decomposes under the prevailing pressures.

REFERENCES:
patent: 3761529 (1973-09-01), Drahoslav et al.
Turova et al., Russian Chemical Reviews, vol. 34(3), pp. 101-163 and 180.
Adickes et al., Berichte, vol. 67, pp. 1436-1440 (1934).

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