Method for the gravimetric determination of oil and grease

Chemistry: analytical and immunological testing – Lubricant – grease – mineral oil – hydrocarbon oil product – or...

Patent

Rate now

  [ 0.00 ] – not rated yet Voters 0   Comments 0

Details

436 8, 73152, 73153, G01N 3100, G01N 3303, G01N 3320

Patent

active

052945537

ABSTRACT:
A non-halogenated solvent mixture for gravimetric determination of grease and oil in an aqueous or a solid matrix comprising a mixture of n-hexane and methyl tertiary-butyl ether present in a volume ratio of 80% to 20% respectively. A method of gravimetric determination of grease and oil in an aqueous or a solid matrix which comprises preparing a sample; extracting the same using this non-halogenated solvent mixture; distilling; evaporating and weighing the extraction residue.

REFERENCES:
patent: 4279664 (1981-07-01), Figiel et al.
patent: 4399693 (1983-08-01), Gournay
patent: 4549966 (1985-10-01), Beall
patent: 4654160 (1987-03-01), Wilson et al.
patent: 4810414 (1989-03-01), Huge-Jensen et al.
patent: 4997243 (1990-12-01), Barder et al.
patent: 5092983 (1992-03-01), Eppig et al.
patent: 5118438 (1992-06-01), Magid et al.
patent: 5128864 (1993-06-01), Pennybaker
The Clean Water Act (CWA) Method 413.1, "Oil and Grease, Total, Recoverable", USEPA, Environmental Monitoring and Support Laboratory, Cincinnati, Ohio 1974.
Standard Method 5520 "Oil and Grease", Standard Methods for the Examination of Water and Wastewater, 17th Ed. (1989), pp. 5-41--5-48.
Kirschman, et al., "Determination of Oil in Oil-Field Waste Waters", Anal. Chem 21, pp. 793-797 (1949).
Gilcreas, F. W., et al., "Two New Methods for the Determination of Grease in Sewage", Sewage and Industrial Wastes, 25, [12] 1379-1390 (1953).
Resource Conservation and Recovery Act Methods (RCRA) 9070A "Total Recoverable Oil and Grease (Gravimetric, Separatory Funnel Extraction)", Rev. 1, Nov. 1990.
Resource Conservation and Recovery Act Methods (RCRA) 9071A "Oil and Grease Extraction Method for Sludge Samples", Rev. 1, Nov. 1990.
Taras et al., "Determination of Emulsifying Oil in Industrial Wastewater", JWPCF Research Suppl., 40, R404-R411 (1968).
Method 502A in "Standard Methods for the Examination of Water and Wastewater," 14th ed., pp. 515-516.
Dr. F. Kawahara, "A Study to Select the Most Suitable Replacement Solvent for Freon 1,1,3 for the Gravimetric Determination of Oil and Grease", Environmental Monitoring Systems Laboratory, 20 pages.
Kawahara, "Study to Determine A Suitable Substitute for Freon 113 in the Gravimetric Analysis of Oil and Grease in Waters".

LandOfFree

Say what you really think

Search LandOfFree.com for the USA inventors and patents. Rate them and share your experience with other people.

Rating

Method for the gravimetric determination of oil and grease does not yet have a rating. At this time, there are no reviews or comments for this patent.

If you have personal experience with Method for the gravimetric determination of oil and grease, we encourage you to share that experience with our LandOfFree.com community. Your opinion is very important and Method for the gravimetric determination of oil and grease will most certainly appreciate the feedback.

Rate now

     

Profile ID: LFUS-PAI-O-1535557

  Search
All data on this website is collected from public sources. Our data reflects the most accurate information available at the time of publication.