Method for the enzymatic racemate resolution of racemic alcohols

Details Method for the enzymatic racemate resolution of racemic alcohols Method for the enzymatic racemate resolution of racemic alcohols

1988-12-21

1990-10-16

Rosen, Sam

Chemistry: molecular biology and microbiology

Process of utilizing an enzyme or micro-organism to destroy...

Resolution of optical isomers or purification of organic...

435155, C12P 702

Patent

active

049634925

ABSTRACT:
Racemic alcohols can be resolved in good yield and with high enantiomeric purity in the presence of vinyl esters with the aid of lipases from pig pancreas, pig liver and microorganisms.

REFERENCES:
patent: 4732853 (1988-03-01), Whitesides et al.
M. Degueil-Castaing et al., "Enzymatic Reactions in Organic Synthesis: 2-Ester Interchange of Vinyl Esters," Tetrahedron Letters, vol. 28, No. 9, 1987, pp. 953-954.
A. Makita et al., "Lipase Catalyzed Synthesis of Macrocyclic Lactones in Organic Solvents," Tetrahedron Letters, vol. 28, No. 7, 1987, pp. 805-808.

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