Method for the continuous preparation of a mixture of a cycloalk

Details Method for the continuous preparation of a mixture of a cycloalk Method for the continuous preparation of a mixture of a cycloalk

1993-12-15

1995-04-11

Reamer, James H.

Organic compounds -- part of the class 532-570 series

Organic compounds

Oxygen containing

568570, 568836, 568821, 568700, C07C 4533

Patent

active

054060010

ABSTRACT:
The present invention relates to a method for the continuous preparation of a mixture of a cycloalkanone, a cycloalkanol and a cycloalkylhydroperoxide. In the method, a cycloalkane, corresponding to the cycloalkenone, cycloalkenol and cycloalkylhydroperoxide, is oxidized in a continuous process, with the aid of an oxygen-containing gas, in the absence of a metal catalyst, at a temperature of between 130.degree. C. and 200.degree. C. The oxidation is at least partly carried out in the presence of between 0.002 and 2 mmol of a phenolic compound per kg of reaction mixture (mmol/kg).

REFERENCES:
patent: 3949004 (1976-04-01), Sorgenti et al.
patent: 5220075 (1993-06-01), Emlen

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