Method for the base-catalyzed decomposition of halogenated and n

Mineral oils: processes and products – Refining – Halogen contaminant removal

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2082621, 208 13, 210909, 134 10, 134 26, 134 27, 134 28, 134 42, 423659, 423DIG20, 502 25, 502 27, 502515, C10G 1700

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050645269

ABSTRACT:
A method for the decomposition of halogenated and non-halogenated organic contaminant compounds contained in a contaminated medium comprises adding an alkali or alkaline earth metal carbonate, bicarbonate or hydroxide to the contaminated medium in an aqueous solution or in a solvent having a boiling point of at least 200.degree. C., or in the form of a solid dispersion or suspension. The medium includes a hydrogen donor compound. The hydrogen donor compound may be originally contained in the medium or may be added to the medium. The medium further includes a catalytic source of carbon, for example, a carabohydrate, which will cause formation of a free radical hydrogen ion from the hydrogen donor compound. The medium is heated to dehydrate the medium and then is further heated at a temperature between about 200.degree. and 400.degree. C. to cause formation of the free radical hydrogen ion and effect reductive decomposition of the halogenated and non-halogenated organic contaminant compounds. An acid is then added to the medium in an amount sufficient to neutralize the same.

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