Method for the automated manufacture of pure SO2 from sulfur...

Chemistry of inorganic compounds – Sulfur or compound thereof – Oxygen containing

Reexamination Certificate

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C423SDIG018, C423SDIG018

Reexamination Certificate

active

07052670

ABSTRACT:
A method for the automated production of liquid SO2having a purity above 99.9% from elemental sulfur and pure oxygen, in the presence of SO2recirculated from a closed circuit production system. The temperature of the combustion is controlled by means of pre-defined S, O2and SO2ratios. The automation is made based on oxygen sensors and on sulfur and SO2flow meters with their respective control connections and proportional valves permitting a fine control of the sulfur combustion reaction. Liquefaction of gaseous SO2produced is carried out alternatively by a cool plant working between −10 and −60° C. or with a compression unit working at a pressure between 3.8 and 5.0 bar. The automation permits an optimum temperature control and a clean production of SO2.

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