Method for testing quality of silicon wafer

Single-crystal – oriented-crystal – and epitaxy growth processes; – Processes of growth from liquid or supercritical state – Having pulling during growth

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117 14, C30B 1500

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053867963

ABSTRACT:
Quick and inexpensive determination of an aggregate of point defects in a grown silicon semiconductor single crystal bar is accomplished by a method which comprises cutting a wafer from a freshly grown silicon single crystal bar, etching the surface of this wafer with the mixture of hydrofluoric acid and nitric acid thereby relieving the wafer of strain, treating the wafer with the mixture of K.sub.2 Cr.sub.2 O.sub.7, hydrofluoric acid, and water thereby giving rise to pits 2 and ripple patterns 1 therein, determining the density of the pits 2 and that of the ripple patterns 1, and rating the aggregate of point defects by virtue of the correlation between the densities of the pits 1 and the ripple patterns 1 and the aggregate of point defects.

REFERENCES:
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patent: 4276114 (1981-06-01), Takano et al.
Journal of the Electrochemical Society, vol. 119, No. 7, (Jul. 1972); pp. 948-951; "Dislocation Etch for (100) Planes in Silicon"; Aragona.
Japanese Journal of Applied Physics, vol. 20, No. 20-2, 1981, pp. 31-37; "Fabrication & Properties of Silicon Solar Cells Using Squarely Shaped Crystals"; Kuroda, et al.
Journal of Applied Physics, vol. 42, No. 11, (Oct. 1971), pp. 4262-4270; "Effect of Growth Parameters on the Residual Stress . . . ", Denicola.
IBM Technical Disclosure Bulletine, vol. 24, No. 18, (Jun. 1981), p. 508; "Crystal Revelation"; Cazcarra.
Applied Physics Letters, (May 1, 1979), pp. 611-613; "The Effect of Doping on Microdefect Formation . . . "; De Kock, et al.
"VLSI Fabrication Principles: Silicon & Gallium Arsenide"; Ghandhi; John Wiley & Sons, Inc., N.Y.; Chapter 9.4 (Cleaning); pp. 517-531 (1983).
"Chemical Etching of Silicon Wafer"; Hamaguchi Journal of the Japan Society of Precision Engineering (May); 1985; vol. 51, No. 5, pp. 1013-1018.

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