Chemistry: electrical and wave energy – Processes and products – Electrostatic field or electrical discharge
Patent
1983-10-28
1985-06-25
Niebling, John F.
Chemistry: electrical and wave energy
Processes and products
Electrostatic field or electrical discharge
204103, C25B 100
Patent
active
045252521
ABSTRACT:
A method and apparatus for electrochemically synthesizing N.sub.2 O.sub.5 includes oxidizing a solution of N.sub.2 O.sub.4 /HNO.sub.3 at an anode, while maintaining a controlled potential between the N.sub.2 O.sub.4 /HNO.sub.3 solution and the anode. A potential of about 1.35 to 2.0 V vs. SCE is preferred, while a potential of about 1.80 V vs. SCE is most preferred. Thereafter, the N.sub.2 O.sub.5 is reacted with either 1.5-diacetyl-3,7-dinitro-1,3,5,7-tetraazacyclooctane (DADN) or 1,3,5,7-tetraacetyl-1,3,5,7-tetraazacyclooctane (TAT) to form cyclotetramethylenetetraamine (HMX).
REFERENCES:
patent: 4443308 (1984-04-01), Coon et al.
J. Zawadski et al, "Electrochemical Preparation of Nitrogen Pentoxide", Rocznki Chemii, 22 (1948), 233.
Coon Clifford L.
Harrar Jackson E.
McGuire Raymond R.
Pearson Richard K.
Davis Paul
Dixon Harold M.
Hightower Judson R.
Niebling John F.
The United States of America as represented by the United States
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