Method for synthesizing aluminum hydride

Chemistry of inorganic compounds – Hydrogen or compound thereof – Binary compound

Patent

Rate now

  [ 0.00 ] – not rated yet Voters 0   Comments 0

Details

25218827, 423497, C01B 600

Patent

active

056701292

ABSTRACT:
The invention relates to a method for the preparation of toluene solutions of aluminum hydride, which is free of ethers and halides, characterized in that the complex, bound magnesium halide portion is precipitated and removed from halogen magnesium aluminum hydridohalides, which optionally are present in tetrahydrofuran (THF) solutions, of the general formula

REFERENCES:
patent: 3758677 (1973-09-01), Kraus et al.
patent: 3801657 (1974-04-01), Scruggs
patent: 3810974 (1974-05-01), King
patent: 3819819 (1974-06-01), Matzek et al.
patent: 3822342 (1974-07-01), Reigler et al.
patent: 3829390 (1974-08-01), Ashby et al.
patent: 3857930 (1974-12-01), Kraus et al.
patent: 3971846 (1976-07-01), Skelcey
patent: 4006095 (1977-02-01), Hoffmann et al.
patent: 4048087 (1977-09-01), Daniels et al.
patent: 4832934 (1989-05-01), Bogdanovic et al.
patent: 5273686 (1993-12-01), Bogdanovic et al.
patent: 5565183 (1996-10-01), Knott
Ullmann's Encyclpedia of Industrial Chemistry, High Performance Fibers to Imidazole and Derivatives, vol. A 13, 213-214.
Finholt, A.E.; Bond, A.C.; and Schlesinger, H.I., Lithium Aluminum Hydride, Aluminum Hydride and Lithium Gallium Hydride, and Some of their Applications in Organic and Inorganic Chemistry, contribution from the George Herbert Jones Laboratory, University of Chicago, vol. 69, 1199-1203 (May 1947).
Ashby, E.C.; Schwartz, R.D.; and James, B.D., Concerning the Preparation of Magnesium Aluminum Hydride. A Study of the Reactions of Lithium and Sodium Aluminum Hydrides with Magnesium Halides in Ether Solvents, contribution from The School of Chemistry, Georgia Institute of Technology, Atlanta, Georgia, vol. 9, No. 2, 325-332(Feb. 1970).

LandOfFree

Say what you really think

Search LandOfFree.com for the USA inventors and patents. Rate them and share your experience with other people.

Rating

Method for synthesizing aluminum hydride does not yet have a rating. At this time, there are no reviews or comments for this patent.

If you have personal experience with Method for synthesizing aluminum hydride, we encourage you to share that experience with our LandOfFree.com community. Your opinion is very important and Method for synthesizing aluminum hydride will most certainly appreciate the feedback.

Rate now

     

Profile ID: LFUS-PAI-O-1937810

  Search
All data on this website is collected from public sources. Our data reflects the most accurate information available at the time of publication.