Method for separating and purifying crystallisable organic...

Synthetic resins or natural rubbers -- part of the class 520 ser – Synthetic resins – Treating polymer containing material or treating a solid...

Reexamination Certificate

Rate now

  [ 0.00 ] – not rated yet Voters 0   Comments 0

Details

C526S348000, C530S344000, C530S412000

Reexamination Certificate

active

08071714

ABSTRACT:
The invention relates to a process for separating and/or purifying organic compounds susceptible to crystallization by means of crystallizing and dissolving comprising the following steps:a) depositing the composition in the head of a separation and/or crystallization column;b) crystallizing by means of a cooling gradient;c) pumping the solvent at optimal flow rate Fc;d) entraining the components while they are not crystallized to the end of the column;e) stopping the pumping of the solvent until reaching the lowest temperature of the interval established by the cooling gradient;f) heating the column;g) beginning new pumping by means of applying flow rate Fe;h) collecting the eluates; andi) detecting by means of detectors.

REFERENCES:
patent: 5008204 (1991-04-01), Stehling
patent: 5222390 (1993-06-01), Monrabal
patent: 0327368 (1989-08-01), None
patent: WO 2004/034047 (2004-04-01), None
Soares et al. “Temperature rising elution fractionation of linear polyolefins.”Polymer. vol. 36. No. 8. 1995. pp. 1639-1654.
Xu et al. “Application of Temperature rising elution fractionation in polyolefins.”European Polymer Journal. vol. 36. 2000. pp. 867-878.
Desreux et al. “Fractionnement par extraction du polythene.”Bull. Soc. Chim. Velg. vol. 59. 1950. pp. 476-489.—English Abstract provided.
Monrabal. “Temperature Rising Elution Fractionation and Crystallization Analysis Fractionation.”Encyclopedia of Analytical Chemistry. John Wily & Sons. 2000. pp. 1-20.
Shirayama et al. “Distribution of Short-Chain Branching in Low-Density Polyethylene.”J. of Polymer Science. Part A. vol.3. 1965. pp. 907-916.
Tung. “Fractionation of Synthetic Polymers: Principles and Practices.”Ed. Marcel Dekker Inc. New York. 1977. pp. 92-93, 102-103, 106-107, 344-345, 498-501, 514-515, 530-531.
Wild et al. “Development of High Performance Tref. For Polyolefin Analysis.”T. C. Chung. Plenum Press. New York. 1993. pp. 147-157.

LandOfFree

Say what you really think

Search LandOfFree.com for the USA inventors and patents. Rate them and share your experience with other people.

Rating

Method for separating and purifying crystallisable organic... does not yet have a rating. At this time, there are no reviews or comments for this patent.

If you have personal experience with Method for separating and purifying crystallisable organic..., we encourage you to share that experience with our LandOfFree.com community. Your opinion is very important and Method for separating and purifying crystallisable organic... will most certainly appreciate the feedback.

Rate now

     

Profile ID: LFUS-PAI-O-4309271

  Search
All data on this website is collected from public sources. Our data reflects the most accurate information available at the time of publication.