Method for separating an esterification catalyst

Catalyst – solid sorbent – or support therefor: product or process – Regenerating or rehabilitating catalyst or sorbent – Treating with a liquid or treating in a liquid phase,...

Reexamination Certificate

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C560S191000

Reexamination Certificate

active

10523284

ABSTRACT:
Process for removal of the esterification catalyst by separation from a crude plasticizer ester obtained by reacting a dicarboxylic acid with C8–C13alcohols, by treating the crude ester with an aqueous alkali solution in the range from 10 to 100° C. and then separating the aqueous alkaline phase comprising the hydrolyzed esterification catalyst by gravitational phase separation, by treating the crude ester, prior to or during the phase separation, with a salt of a di- or polyvalent metal, or with a mixture of these salts.

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patent: 26 12 355 (1977-10-01), None
patent: 197 21 347 (1998-11-01), None
patent: 1030214 (1966-05-01), None

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