Method for separating an azepine derivative out of a mixture...

Distillation: processes – separatory – With measuring – testing or inspecting – Of temperature or pressure

Reexamination Certificate

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C203S049000, C203S075000, C203S077000, C203S078000, C203S080000, C203SDIG025, C540S605000, C540S612000, C558S452000, C564S437000, C564S497000

Reexamination Certificate

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07147757

ABSTRACT:
The invention relates to a method for separating by distillation a portion or the entirety of an azeptine derivative (III), which is selected from the group consisting of aminohexylidene imine, tetrahydroazepine, hexylhexahydroazepine and of aminohexylhexahydroazepine, out of a mixture (II) containing an azepine derivative (III) and an amine (I). The inventive method is characterized in that the distillation is carried out with a maximum bottom temperature of 150° C.

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patent: 2762835 (1956-09-01), Swerdloff
patent: 4110326 (1978-08-01), Tuba et al.
patent: 5192399 (1993-03-01), Sieja
patent: 5717090 (1998-02-01), Bassler et al.
patent: 6204408 (2001-03-01), Bassler et al.
patent: 6252115 (2001-06-01), Luyken et al.
patent: 6300497 (2001-10-01), Rehfinger et al.
patent: 6649799 (2003-11-01), Ostgard et al.
patent: 198 39 338 (2000-03-01), None

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